Intensity Correction and Pole Figure Measurement of Copper Metallic by XRD
PDF

Keywords

 X-ray diffraction, intensity correction, pole figure.

How to Cite

Halo Dalshad Omar. (2016). Intensity Correction and Pole Figure Measurement of Copper Metallic by XRD. Journal of Basic & Applied Sciences, 12, 320–322. https://doi.org/10.6000/1927-5129.2016.12.49

Abstract

In this research work the process of data intensity correction and pole figure measurement were investigated and analyzed by using X-Ray Diffraction (XRD) technique. Different corrections were studied, to see their influence on the crystallographic texture analysis. Specific software, which is Labotex was used to determine the pole figure for copper (Cu) metallic after which the data corrections have been made. The copper, Cu sample was simply prepared by a low cost method Mini Mill 2 Panalytical and the sample was rotated for 10 minutes by grinding the sample at high speed of 250 rpm.

https://doi.org/10.6000/1927-5129.2016.12.49
PDF

References

Ostafin M, Pospiech J, Schwarzer RA. Microstructure and Texture in Copper Sheets after Reverse and Cross Rolling. J Scient 2005; 105: 309-314. http://dx.doi.org/10.4028/www.scientific.net/ssp.105.309

Faurie D, Renault P-O, Le Bourhis E, Goudeau Ph. Determination of elastic constants of a fiber-textured gold film by combining synchrotron x-ray diffraction and in situ tensile testing. J Appl Phys 2005; 98: 093511. http://dx.doi.org/10.1063/1.2126154

Hong B, Jiang C-H, Wang X-J. Texture of Electroplated Copper Film under Biaxial Stress. Mater Trans 2006; 47: 2299-2301. http://dx.doi.org/10.2320/matertrans.47.2299

Palacios G´omez J, SalatFigols RS, Jim´enez Jim´enez A, Kryshtab T. Contributions to the defocusing effect on pole figure measurements by X-ray diffraction. Revista Mexicana de F´?sica 2015; 61: 296-300.

Siemes H, Rosire CA, Hackspacher P, Schafer W, Jansen E. Defocusing correction of X-ray pole figures by means of neutron pole figure measurement. Textures and Microstructures 1999; 34: 55-62. http://dx.doi.org/10.1155/TSM.34.55

Fanxiong, Parker BA. The Determination of Complete Pole Figures Using the Reflection Method, Textures and Microstructures. Gordon and Breach Science Publishers Inc. and OPA Ltd. 1984; 6: 125-136.

X-ray texture analysis in films by the reflection method: Principle aspects and applications. Materials Science Forum 1994; 157: 1379-1386.

Wenk H-R, Matthies S, Donovan J, Chateigner D. Beartex. a Windows-based program system for quantitative texture analysis. J Appl Cryst 1998; 31: 262-269. http://dx.doi.org/10.1107/S002188989700811X

Liu YS, Depre L, de Buyser L, Wu TB, Vanhoutte P. Intensity correction in texture measurement of polycrystalline thin films by X-ray diffraction. J Taylor Francis 2003; 35: 283-290. http://dx.doi.org/10.1080/07303300310001597035

Kocks UF, Tome CN, Wenk H-R. Texture and Anisotropy, Cambridge, 1998.

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

Copyright (c) 2016 Halo Dalshad Omar